Preconcentration and Determination of Iron, Nickel, Lead and Zinc after Solid Phase Extraction using 5-Aphen Functionalized poly(GMA-MMA-DVB) Microspheres

ALPDOĞAN G., Yamak H., Zor S. D., Elmali F.

CURRENT ANALYTICAL CHEMISTRY, cilt.12, sa.5, ss.500-509, 2016 (SCI-Expanded) identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 12 Sayı: 5
  • Basım Tarihi: 2016
  • Doi Numarası: 10.2174/1573411012666160616105850
  • Dergi Adı: CURRENT ANALYTICAL CHEMISTRY
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Sayfa Sayıları: ss.500-509
  • Anahtar Kelimeler: 5-Aphen, glycidylmethacrylate copolymer, solid phase extraction, trace metal determination, FAAS, herbal tea, ATOMIC-ABSORPTION-SPECTROMETRY, TRACE-METAL IONS, XAD-16 CHELATING RESIN, CLOUD POINT EXTRACTION, WATER SAMPLES, HEAVY-METALS, ENVIRONMENTAL-SAMPLES, EMISSION-SPECTROMETRY, MODIFIED ELECTRODES, BIOLOGICAL SAMPLES
  • Yıldız Teknik Üniversitesi Adresli: Evet

Özet

Background: Polymer based adsorbents and their modified forms by various ligands have been effectively used for separation, preconcentration, determination and removal of heavy metal ions from different matrices. This paper proposes a solid phase extraction method based on 5-amino-1,10-phenanthroline (5-Aphen) functionalized glycidyl methacrylate-methyl methacrylate-divinylbenzene (GMA-MMA-DVB) crosslinked-polymeric microspheres for the determination of Fe (II), Ni (II), Pb (II) and Zn (II) in herbal tea samples employing flame atomic absorption spectrometry (FAAS).