Sensitive, Accurate and Selective Determination of Cd(II) Using Anodic Stripping Voltammetry With In-situ Hg-Bi Film Modified Pencil Graphite Electrode After Magnetic Dispersive Solid Phase Microextraction

Yaman B., Zaman B. T., BAKIRDERE S., DİLGİN Y.

ELECTROANALYSIS, cilt.33, sa.10, ss.2161-2168, 2021 (SCI-Expanded) identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 33 Sayı: 10
  • Basım Tarihi: 2021
  • Doi Numarası: 10.1002/elan.202100228
  • Dergi Adı: ELECTROANALYSIS
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus, Academic Search Premier, Aerospace Database, Applied Science & Technology Source, BIOSIS, Chemical Abstracts Core, Chimica, Communication Abstracts, Metadex, Civil Engineering Abstracts
  • Sayfa Sayıları: ss.2161-2168
  • Anahtar Kelimeler: Cadmium, dispersive solid phase microextraction, stripping voltammetry, magnetic nanoparticles, graphite pencil electrode, EXTRACTION
  • Yıldız Teknik Üniversitesi Adresli: Evet

Özet

This paper describes a novel approach to detect Cd(II) using the combination of the differential pulse anodic stripping voltammetry and magnetic nanoparticle based dispersive solid phase microextraction as an efficient, green and accurate method. Currents of Cd(II) increased linearly in the range from 75 to 2000 ngL(-1) Cd(II) with a detection limit of 21.6 ngL(-1). The RSD values of 2.6 and 6.0 % for 1.00 and 0.10 mu g L-1 respectively showed that proposed method has an acceptable repeatability. Recovery values between 92.3 and 98.6 % showed that this approach can be successfully used for determination of Cd(II) in water samples.