Solid phase extraction of Cu (II), Ni (II), Co (II), and Fe (III) ions in water samples using salicylaldehyde benzoylhydrazone on Amberlite XAD-4 and their determinations by flame atomic absorption spectrometry

ALPDOĞAN, Güzin

doi:10.1080/02772248.2015.1115508

Solid phase extraction of Cu (II), Ni (II), Co (II), and Fe (III) ions in water samples using salicylaldehyde benzoylhydrazone on Amberlite XAD-4 and their determinations by flame atomic absorption spectrometry

Atıf İçin Kopyala

ALPDOĞAN G.

TOXICOLOGICAL AND ENVIRONMENTAL CHEMISTRY, cilt.98, sa.2, ss.179-188, 2016 (SCI-Expanded)

Yayın Türü: Makale / Tam Makale
Cilt numarası: 98 Sayı: 2
Basım Tarihi: 2016
Doi Numarası: 10.1080/02772248.2015.1115508
Dergi Adı: TOXICOLOGICAL AND ENVIRONMENTAL CHEMISTRY
Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
Sayfa Sayıları: ss.179-188
Yıldız Teknik Üniversitesi Adresli: Evet

Özet

A multi element preconcentration procedure for solid phase extraction on Amberlite XAD-4 as their salicylaldehyde benzoylhydrazone chelates and flame atomic absorption spectrometric determination of some trace metal ions in water samples are proposed in this work. The influences of some analytical parameters, including pH of aqueous solution, amounts of reagent, flow rates of sample and eluent solutions, and sample volume on the quantitative recoveries of copper, nickel, cobalt, and iron were investigated. The effects of concomitant ions on the retentions of the analytes were also examined. The developed method has been successfully applied to the determination of metal ions in some real samples, including, tap water, river water, spring water, and waste water.